Potassium chloride for industrial use — Determination of potassium content — Flame emission spectrop...
Is applicable to products having a minimum KCl content of about 95 % (m/m). The principle consists in dissolution of a test portion taken from the laboratory sample, previously ground and sifted. Acidification to pH 1 after suitable dilution, and atomization of the resultant solution in the burner of a flame spectrophotometer. Measurement of the intensity of the 766 nm ray, compared with the…
Potassium chloride for industrial use — Determination of potassium content — Potassium tetraphenylbo...
The method is applicable to products having a minimum KCL content of about 95 % (m/m). The principle consists in dissolution of a test portion taken from the laboratory sample, previously ground and sifted. Addition of formaldehyde solution to transform any ammonium ions present into hexamethylenetetramine, and of ethylenedinitrilotetraacetic acid, disodium salt, to complex any extraneous cations…
Potassium chloride for industrial use — Determination of potassium content — Sodium tetraphenylborat...
The method is applicable to products having a minimum KCl content of about 95 % (m/m). The principle consists in dissolution of a test portion taken from the previously ground and sifted laboratory sample and elimination of many ammonium ions present. Precipitation of the potassium, in a slightly acid medium, by an excess of an standard volumetric sodium tetraphenylborate solution. Filtration and…
Three types of crucibels are specified: Type 1, low form, type 2 medium form and type 3 tall form bases an a height/diameter ratio of 0,63; 0,8 and 1,25 resp. Further two types of lid are described: type D, a lid of slightly domed shape and typ R, a recessed lid. Material and construction are specified, shape and dimensions are shown in drawings and in a table.
Porcelain laboratory apparatus — Requirements and methods of test
The requirements specify the quality of the material. The different methods of test are specified. They concern the porosity and imperfections of glaze, the resistance to heat and sudden change in temperature, the resistance of glaze to high temperature, to acid and to alkali and the constancy of mass on ignition.
A system of color coding is specified for one-mark pipettes for identification of nominal capacities, and for graduated pipettes for identification of nominal capacities and unit of subdivision. The color code bands for the different capacities are tabled and the method of marking is specified. Suitable requirements and test methods for the durability of the colours are intended to be considered…
The requirements deal with the geometric charateristics to ensure interchangeability. The dimensions of the joint-ground zone and the outer diameter of the tube connected to the joint are given in a table and illustrated in a drawing. In addition the surface finish is specified. A system of gauges (stell balls) for testing the ball cup is tabled. In the annex a method of testing the leakage…
Statistical interpretation of data — Comparison of two means in the case of paired observations
A method is specified for comparing the mean of a population of differences with zero or any other preassigned value. It may be applied to establish a difference between two treatments, where "treatment" should be understood in a wide sense, e.g. as a test method, measuring instrument or laboratory involved, and is applicable under the conditions that the series of differences can be…
Anhydrous hydrogen fluoride for industrial use — Sampling
This part contains a method for taking laboratory samples intended for the determination of the water content and the preparations of the test samples. Contains instructions for handling with the material. Applicable for taking samples of this highly corrosive liquid from road and rail tanks, drums and cylinders. The principle consists in allowing the liquid of one of these containers to flow in…
