Should be read in conjunction with ISO 4297. Specifies principle, reagents, apparatus, sample, procedure and expression of results. A figure gives an example of apparatus.
Condensed phosphates for industrial use (including foodstuffs) — Determination of calcium content — ...
Applicable to products having Ca contents equal to or more than 50 mg/kg. The presence of soluble SiO2 up to 5 g/ml in the test solution does not interfere. Hydrolysis by boiling a test portion in hydrochloric acid medium. Addition of sodium ions, until a constant concentration is obtained, to stabilize the promotion and emission of Ca; addition of lanthanum chloride to increase the sensitivity…
Acetic acid for industrial use — Methods of test — Part 4: Determination of acetaldehyde monomer con...
The principle of the determination consists in reaction of the acetaldehyde present in a test portion with an excess of sodium hydrogen sulphite solution, and iodometric titration of the residual sodium hydrogen sulphite. The method is applicable to products having acetaldehyde monomer contents equal to or greater than 0,01 % (m/m). This International Standard as also been approved by the…
Acetic acid for industrial use — Methods of test — Part 5: Determination of total acetaldehyde conte...
The method specified consists in heating a test portion in an acid medium to depolymerize any to paraldehyde present and to entrain, by distillation, both regenerated acetaldehyde and the monomeric acetaldehyde originally present. Reaction of the acetaldehyde in the distillate with an excess of sodium hydrogen sulphite solution. Iodometric titration of the residual sodium hydrogen sulphite…
Acetic acid for industrial use — Methods of test — Part 8: Visual limit test for inorganic chlorides
Specifies a method for a visual comparison of the tubitity obtained by adding a silver nitrate solution to a solution of a test portion acidified with nitric acid, with that similary obtained from a chloride solution of known concentration. Using a test portion of 50 g, the method is applicable directly to products having inorganic chloride contents in the range 0,0005 % (m/m) to 0,05 % (m/m).…
Acetic acid for industrial use — Methods of test — Part 9: Visual limit test for inorganic sulphates
Specifies a method for a visual comparison of the turbitity obtained by adding a barium chloride solution to a solution of a test portion acidified with hydrochloric acid, with that similarly obtained from a sulphate solution of known concentration. Using a test portion of 100 g, the method is applicable directly to products having inorganic sulphate contents in the range 0,001 % (m/m) to 0,1 % (…
Acetic acid for industrial use — Methods of test — Part 10: Visual limit test for heavy metals (incl...
The principle consists in conversion of heavy metals, such as lead, copper and iron, to their sulphides by treatment with sodium sulphide in ammoniacal solution, and visual comparison of the colour produced with that of a standard lead solution similarly treated. The method detects only the heavy metals present in non-complex form. Using a test portion of 25 g, the method is applicable directly…
Acetic acid for industrial use — Methods of test — Part 1: General
Gives general instructions and also specifies the methods to be used for the determination of dry residue after evaporation on a water bath, for the determination of the crystallizing point (temperature) of glacial acetic acid, for the determination of water content, for the measurement of colour and for the determination of arsenic content. The method is applicable to products having acedic acid…
Acetic acid for industrial use — Method of test — Part 2: Determination of acetic acid content — Tit...
The principle consists in titration of a test portion with standard volumetric sodium hydroxide solution, using phenolphthalein as indicator. Calculation of the acid content, making allowance for any formic acid present, determined separately (see ISO 753/3). This International Standard has also been approved by the International Union of Pure and Applied Chemistry (IUPAC). International…
